Intshayelelo kwi-Small Peptide Trace Mineral Chelates
Icandelo 1 Imbali yezongezo zeminerali ezilandelelanayo
Ingohlulwa ibe zizizukulwana ezine ngokwendlela eziphuhliswe ngayo izongezo zeminerali ezilandelelanayo:
Isizukulwana sokuqala: Iityuwa ze-inorganic zeeminerali ezilandelelanayo, ezifana ne-copper sulfate, i-ferrous sulfate, i-zinc oxide, njl.njl.; Isizukulwana sesibini: Iityuwa ze-organic acid zeeminerali ezilandelelanayo, ezifana ne-ferrous lactate, i-ferrous fumarate, i-copper citrate, njl.njl.; Isizukulwana sesithathu: Uhlobo lokutya lwe-amino acid chelate yeeminerali ezilandelelanayo, ezifana ne-zinc methionine, i-iron glycine kunye ne-zinc glycine; Isizukulwana sesine: Iityuwa zeproteni kunye neetyuwa ze-peptide chelating ezincinci zeeminerali ezilandelelanayo, ezifana ne-protein copper, i-protein iron, i-protein zinc, i-protein manganese, i-small peptide copper, i-small peptide iron, i-small peptide zinc, i-small peptide manganese, njl.njl.
Isizukulwana sokuqala ziiminerali ezingabonakaliyo, kwaye isizukulwana sesibini ukuya kwesesine ziiminerali ezingabonakaliyo.
Icandelo 2 Kutheni Ufanele Ukhethe iiChelates zePeptide ezincinci
Ii-chelates zepeptide ezincinci zisebenza ngolu hlobo lulandelayo:
1. Xa iipeptides ezincinci zixubana nee-ion zesinyithi, zizityebi kwiifom kwaye kunzima ukuzigcwalisa;
2. Ayikhuphisani nemijelo ye-amino acid, ineendawo ezininzi zokufunxa kunye nesantya sokufunxa ngokukhawuleza;
3. Ukusetyenziswa kwamandla okuncinci; 4. Iidiphozithi ezingaphezulu, izinga eliphezulu lokusetyenziswa kunye nokusebenza kakuhle kwemveliso yezilwanyana;
5. Ilwa neentsholongwane kunye ne-antioxidant;
6. Ulawulo lomzimba olulawulayo.
Inani elikhulu lezifundo libonise ukuba ezi mpawu okanye iziphumo ze-peptide chelates ezincinci zenza ukuba zibe namathuba amaninzi okusetyenziswa kunye namathuba ophuhliso, ngoko ke inkampani yethu ekugqibeleni igqibe ekubeni ithathe i-peptide chelates ezincinci njengeyona nto iphambili kuphando nophuhliso lwemveliso ye-organic trace mineral yenkampani.
Icandelo 3 Ukusebenza kakuhle kwee-chelates ze-peptide ezincinci
1. Ubudlelwane phakathi kweepeptides, ii-amino acids kunye neeproteni
Ubunzima be-molecular yeprotheni bungaphezulu kwe-10000;
Ubunzima bemolekyuli yepeptide yi-150 ~ 10000;
Iipeptides ezincinci, ezikwabizwa ngokuba ziipeptides ezincinci zemolekyuli, ziqulathe ii-amino acids ezi-2 ukuya kwezi-4;
Ubunzima obuqhelekileyo bee-amino acids bumalunga ne-150.
2. Ukulungelelanisa amaqela ee-amino acids kunye neepeptides ezixutywe neesinyithi
(1) Amaqela adibanisayo kwii-amino acids
Amaqela okulungelelanisa kwii-amino acids:
Amaqela e-amino kunye ne-carboxyl kwi-a-carbon;
Amaqela ee-amino acids ezikwicala elinye, njenge-sulfhydryl group ye-cysteine, i-phenolic group ye-tyrosine kunye ne-imidazole group ye-histidine.
(2) Amaqela aququzelelayo kwiipeptides ezincinci
Iipeptides ezincinci zinamaqela adibanisayo amaninzi kunee-amino acids. Xa zixubana nee-ion zesinyithi, kulula ukuzixubana, kwaye zinokwenza i-multidentate chelation, nto leyo eyenza i-chelate izinze ngakumbi.
3. Ukusebenza kakuhle kwemveliso ye-peptide chelate encinci
Isiseko sethiyori se-peptide encinci ekhuthaza ukufunxwa kweeminerali ezilandelelanayo
Iimpawu zokufunxwa kweepeptides ezincinci zisisiseko sethiyori sokukhuthaza ukufunxwa kwezinto ezilandelelanayo. Ngokwethiyori yesiqhelo yeproteni metabolism, oko izilwanyana zikufunayo kwiproteni koko zikufunayo kwiiamino acids ezahlukeneyo. Nangona kunjalo, kwiminyaka yakutshanje, izifundo zibonise ukuba umlinganiselo wokusetyenziswa kweeamino acids kwizondlo ezivela kwimithombo eyahlukeneyo wahlukile, kwaye xa izilwanyana zondliwa ngokutya okune-homozygous okanye ukutya okune-protein amino acid elinganiselayo ephantsi, ukusebenza kwemveliso engcono kakhulu akunakufumaneka (Baker, 1977; Pinchasov et al., 1990) [2,3]. Ke ngoko, ezinye iingcali zibeka phambili umbono wokuba izilwanyana zinamandla akhethekileyo okufunxwa kwiproteni engapheliyo okanye iipeptides ezinxulumene nayo. U-Agar (1953)[4] waqala waphawula ukuba indlela yamathumbu inokufunxwa kwaye ithuthe i-diglycidyl ngokupheleleyo. Ukususela ngoko, abaphandi babeke phambili ingxoxo ekholisayo yokuba iipeptides ezincinci zinokufunxwa ngokupheleleyo, ziqinisekisa ukuba i-glycylglycine engapheliyo iyathuthwa kwaye ifunxwe; Inani elikhulu leepeptides ezincinci zinokufunxwa ngqo kwi-systemic circulation ngendlela yeepeptides. UHara et al. (1984)[5] ukwabonise ukuba iimveliso zokugaya zeproteni kwindlela yokugaya ikakhulu ziipeptides ezincinci kunee-amino acids zasimahla (FAA). Iipeptides ezincinci zinokudlula kwiiseli ze-mucosal zamathumbu ngokupheleleyo kwaye zingene kwi-systemic circulation (Le Guowei, 1996)[6].
Inkqubela yoPhando lwePeptide encinci ekhuthaza ukufunxwa kweeMbiwa eziLahlekileyo, uQiao Wei, et al.
Ii-chelates ze-peptide ezincinci ziyathuthwa kwaye zifunxwe ngendlela yee-peptides ezincinci
Ngokwendlela yokufunxa kunye nokuthutha kunye neempawu zeepeptides ezincinci, iiminerali ezincinci zixubana neepeptides ezincinci njengoko iiligands eziphambili zinokuthuthwa zizonke, nto leyo enceda ngakumbi ekuphuculeni amandla ebhayoloji eeminerali ezincinci. (Qiao Wei, et al)
Ukusebenza kakuhle kweChelates zePeptide ezincinci
1. Xa iipeptides ezincinci zixubana nee-ion zesinyithi, zizityebi kwiifom kwaye kunzima ukuzigcwalisa;
2. Ayikhuphisani nemijelo ye-amino acid, ineendawo ezininzi zokufunxa kunye nesantya sokufunxa ngokukhawuleza;
3. Ukusetyenziswa kwamandla amancinci;
4. Iidiphozithi ezingaphezulu, izinga eliphezulu lokusetyenziswa kunye nokusebenza ngcono kakhulu kwemveliso yezilwanyana;
5. Ilwa neentsholongwane kunye ne-antioxidant; 6. Ukulawulwa komzimba.
4. Ukuqonda okungakumbi ngeepeptides
Ngowuphi kwaba basebenzisi be-peptide ababini ofumana inzuzo engaphezulu?
- I-peptide ebophayo
- I-Phosphopeptide
- Izinto ezisetyenziswayo ezinxulumene noko
- I-peptide ye-antimicrobial
- I-peptide yomzimba
- I-Neuropeptide
- I-peptide yehomoni
- I-peptide ye-Antioxidant
- Iipeptides zesondlo
- Iipeptides zokuqhola
(1) Ukuhlelwa kweepeptides
(2) Iziphumo ze-peptides kwi-physiological
- 1. Lungisa ibhalansi yamanzi kunye ne-electrolyte emzimbeni;
- 2. Yenza ii-antibodies ezilwa neebhaktheriya kunye neentsholongwane ukuze inkqubo yomzimba yokuzikhusela iphucule ukusebenza kwayo;
- 3. Ukukhuthaza ukuphiliswa kwenxeba; Ukulungiswa ngokukhawuleza kokulimala kwezicubu ze-epithelial.
- 4. Ukwenza ii-enzymes emzimbeni kunceda ukuguqula ukutya kube ngamandla;
- 5. Ukulungisa iiseli, ukuphucula imetabolism yeeseli, ukuthintela ukuwohloka kweeseli, kunye nokudlala indima ekuthinteleni umhlaza;
- 6. Ukukhuthaza ukwenziwa kunye nokulawulwa kweeproteni kunye nee-enzymes;
- 7. Isithunywa esibalulekileyo seekhemikhali sokunxibelelana ngolwazi phakathi kweeseli kunye namalungu omzimba;
- 8. Ukuthintela izifo zentliziyo kunye nemithambo yegazi;
- 9. Lawula iinkqubo ze-endocrine kunye ne-nervous.
- 10. Ukuphucula indlela yokugaya ukutya kunye nokunyanga izifo ezingapheliyo zesisu;
- 11. Ukuphucula isifo seswekile, isifo samathambo, isifo samathambo nezinye izifo.
- 12. Usulelo oluchasene neentsholongwane, oluchasene nokwaluphala, ukususwa kwee-free radicals ezigqithisileyo emzimbeni.
- 13. Ukukhuthaza ukusebenza kwe-hematopoietic, ukunyanga i-anemia, ukuthintela ukuhlangana kweeplatelet, okunokuphucula amandla okuthwala ioksijini kwiiseli ezibomvu zegazi.
- 14. Ukulwa ngokuthe ngqo neentsholongwane ze-DNA kunye neentsholongwane ezihlaselayo.
5. Umsebenzi ophindwe kabini wesondlo se-peptide chelates encinci
I-peptide chelate encinci ingena kwiseli iyonke emzimbeni wesilwanyana, kwayeemva koko yaphula ngokuzenzekelayo ibhondi ye-chelationkwiseli ize ibole ibe zii-ion ze-peptide kunye nezesinyithi, ezisetyenziswa ngokulandelelanayo yi-isilwanyana sidlala imisebenzi emibini yesondlo, ngakumbi iindima yokusebenza kwepeptide.
Umsebenzi we-peptide encinci
- 1. Khuthaza ukwenziwa kweproteni kwizicubu zemisipha yezilwanyana, ukunciphisa i-apoptosis, kunye nokukhuthaza ukukhula kwezilwanyana
- 2.Phucula isakhiwo sezityalo zamathumbu kwaye ukhuthaze impilo yamathumbu
- 3. Ukubonelela nge-carbon skeleton kwaye wonyuse umsebenzi wee-enzymes zokugaya ukutya ezifana ne-amylase yamathumbu kunye ne-protease
- 4.Ineziphumo zoxinzelelo lwe-anti-oxidative
- 5. Uneempawu zokulwa nokuvuvukala
- 6.……
6. Iingenelo ze-chelates ezincinci ze-peptide kune-chelates ze-amino acid
| Iiminerali ezincitshisiweyo ze-amino acid | Iiminerali ezincinci ze-peptide chelated trace | |
| Ixabiso lezinto eziluhlaza | Izinto ezisetyenziswa kwi-amino acid enye zibiza kakhulu | Izinto ezisetyenziswa eTshayina njengekeratin zininzi. Iinwele, iimpuphu kunye neempondo ekufuyweni kwezilwanyana kunye namanzi amdaka eproteni kunye neengceba zesikhumba kwishishini leekhemikhali zizinto ezisetyenziswa eproteni ezikumgangatho ophezulu nezingabizi kakhulu. |
| Isiphumo sokufunxa | Amaqela e-amino kunye ne-carboxyl abandakanyeka ngaxeshanye ekuqhekekeni kwee-amino acids kunye nezinto zesinyithi, zenza isakhiwo se-bicyclic endocannabinoid esifana nese-dipeptides, kungekho maqela e-carboxyl akhululekileyo, anokufunxwa kuphela ngenkqubo ye-oligopeptide. (Su Chunyang et al., 2002) | Xa iipeptides ezincinci zithatha inxaxheba kwi-chelation, isakhiwo se-single ring chelation sidla ngokwenziwa liqela le-terminal amino kunye ne-peptide bond oxygen esecaleni, kwaye i-chelate igcina iqela le-carboxyl elikhululekileyo, elinokufunxwa ngenkqubo ye-dipeptide, ngokuqina okuphezulu kokufunxwa kunenkqubo ye-oligopeptide. |
| Uzinzo | Ii-ion zesinyithi ezinezangqa ezinelungu elinye okanye ngaphezulu ezinamalungu amahlanu okanye amathandathu zamaqela e-amino, amaqela e-carboxyl, amaqela e-imidazole, amaqela e-phenol, kunye namaqela e-sulfhydryl. | Ukongeza kumaqela amahlanu akhoyo okulungelelanisa ii-amino acids, amaqela e-carbonyl kunye ne-imino kwiipeptides ezincinci nawo anokubandakanyeka ekudibaniseni, ngaloo ndlela enza ii-chelate ze-peptides ezincinci zizinzile ngakumbi kunee-chelate ze-amino acid. (Yang Pin et al., 2002) |
7. Iingenelo ze-chelates ezincinci ze-peptide kune-glycolic acid kunye ne-methionine chelates
| Iiminerali zeGlycine chelated trace | Iiminerali ze-methionine chelated trace | Iiminerali ezincinci ze-peptide chelated trace | |
| Ifomu yokulungelelanisa | Amaqela e-carboxyl kunye nama-amino e-glycine anokuhlanganiswa nee-ion zesinyithi. | Amaqela e-carboxyl kunye nama-amino e-methionine anokuhlanganiswa nee-ion zesinyithi. | Xa ixutywe nee-ion zesinyithi, ityebile kwiindlela zokudibanisa kwaye ayigcwali lula. |
| Umsebenzi wesondlo | Iindidi kunye nemisebenzi yee-amino acids ziyafana. | Iindidi kunye nemisebenzi yee-amino acids ziyafana. | Iiintlobo ezahlukeneyo ezityebileyoii-amino acids zibonelela ngesondlo esipheleleyo, ngelixa iipeptides ezincinci zinokusebenza ngokufanelekileyo. |
| Isiphumo sokufunxa | Ii-chelates zeGlycine zinayonoamaqela e-carboxyl akhululekileyo akhona kwaye anefuthe lokufunxa kancinci. | Ii-chelates zeMethionine zinenoamaqela e-carboxyl akhululekileyo akhona kwaye anefuthe lokufunxa kancinci. | Ii-peptide chelates ezincinci ezenziweyoqulathaubukho bamaqela e-carboxyl akhululekileyo kwaye banefuthe lokufunxa ngokukhawuleza. |
Icandelo lesi-4 Igama loRhwebo “IiChelates ezincinci zePeptide-mineral”
IiChelates ezincinci zePeptide-mineral, njengoko igama lisitsho, kulula ukuzicola.
Ithetha ii-peptide ligands ezincinci, ezingagcwali lula ngenxa yenani elikhulu lamaqela adibanisayo, Kulula ukwenza i-multidentate chelate enezinto zesinyithi, enozinzo oluhle.
Icandelo lesi-5 Intshayelelo kwiimveliso zeChelates Series zePeptide-mineral Small
1. I-minerali encinci ye-peptide trace ye-copper e-chelated copper (igama lorhwebo: i-Copper Amino Acid Chelate Feed Grade)
2. I-iron etyheliweyo ye-peptide encinci (igama lorhwebo: I-Ferrous Amino Acid Chelate Feed Grade)
3. Iminerali encinci ye-peptide trace ye-zinc etyheliweyo (igama lorhwebo: i-Zinc Amino Acid Chelate Feed Grade)
4. Iminerali encinci ye-peptide trace ye-manganese etyheliweyo (igama lorhwebo: iManganese Amino Acid Chelate Feed Grade)
Ibanga lokutya leCopper Amino Acid Chelate
Udidi lokutya lweFerrous Amino Acid Chelate
Ibanga lokutya le-Zinc Amino Acid Chelate
Ibanga lokutya leManganese Amino Acid Chelate
1. Udidi lokutya lweCopper Amino Acid Chelate
- Igama leMveliso: Ibanga lokutya leCopper Amino Acid Chelate
- Inkangeleko: Iigranule eziluhlaza ezimdaka
- Iiparamitha zefiziksikhemikhali
a) Ubhedu: ≥ 10.0%
b) Ii-amino acids zizonke: ≥ 20.0%
c) Izinga le-Chelation: ≥ 95%
d) I-Arsenic: ≤ 2 mg/kg
e) I-Lead: ≤ 5 mg/kg
f) I-Cadmium: ≤ 5 mg/kg
g) Umxholo wokufuma: ≤ 5.0%
h) Ubunono: Zonke iisuntswana zidlula kwi-mesh ezingama-20, kunye nobukhulu beesuntswana eziyintloko eziyi-mesh ezingama-60-80
n=0,1,2,... ibonisa i-chelated copper kwi-dipeptides, ii-tripeptides, kunye nee-tetrapeptides
I-Diglycerin
Ulwakhiwo lwee-chelates ze-peptide ezincinci
Iimpawu zeCopper Amino Acid Chelate Feed Grade
- Le mveliso yiminerali ephilayo yonke e-chelating eyenziwe ngenkqubo ekhethekileyo ye-chelating ene-enzyme yezityalo ezincinci ze-peptides njenge-chelating substrates kunye nezinto ezilandelelanayo.
- Le mveliso izinzile ngokweekhemikhali kwaye inokunciphisa kakhulu umonakalo wayo kwiivithamini kunye namafutha, njl.
- Ukusetyenziswa kwale mveliso kuyanceda ekuphuculeni umgangatho wesondlo. Imveliso ifunxwa ngeendlela ezincinci zepeptide kunye ne-amino acid, kunciphisa ukhuphiswano kunye nokuchasana nezinye izinto ezincinci, kwaye inezinga eliphezulu lokufunxwa kunye nokusetyenziswa kwe-bio.
- Ubhedu yinxalenye ephambili yeeseli ezibomvu zegazi, izicwili ezidityanisiweyo, amathambo, abandakanyekayo emzimbeni weentlobo ngeentlobo zee-enzymes, aphucula umsebenzi womzimba wokuzikhusela, isiphumo se-antibiotic, inokunyusa ukutyeba kwemihla ngemihla, iphucule umvuzo wesondlo.
Ukusetyenziswa kunye nokusebenza kakuhle kweCopper Amino Acid Chelate Feed Grade
| Into yesicelo | Idosi ecetyiswayo (izinto ezixabisekileyo ngokupheleleyo ze-g/t) | Umxholo kwi-feed epheleleyo (mg/kg) | Ukusebenza kakuhle |
| Hlwayela | 400～700 | 60～105 | 1. Ukuphucula ukusebenza kokuzala kunye neminyaka yokusebenzisa iimazi; 2. Yandisa amandla eemveku kunye neehagu ezincinci; 3. Ukuphucula amajoni omzimba kunye nokumelana nezifo. |
| Intshontsho lehagu | 300～600 | 45～90 | 1. Iluncedo ekuphuculeni imisebenzi ye-hematopoietic kunye ne-immune system, iphucula ukumelana noxinzelelo kunye nokumelana nezifo; 2. Ukwandisa izinga lokukhula kunye nokuphucula kakhulu ukusebenza kakuhle kokutya. |
| Iihagu ezityebisayo | 125 | 18.5 kaJanuwari | |
| Intaka | 125 | 18.5 kaJanuwari | 1. Ukuphucula ukumelana noxinzelelo kunye nokunciphisa ukufa; 2. Ukuphucula ukubuyiswa kokutya kunye nokwandisa izinga lokukhula. |
| Izilwanyana zasemanzini | Intlanzi 40～70 | 6～10.5 | 1. Khuthaza ukukhula, uphucule ukubuyiswa kokutya; 2. Ukulwa noxinzelelo, ukunciphisa ukugula nokufa. |
| I-Shrimp 150～200 | 22.5～30 | ||
| Isilwanyana esizingelayo g/intloko yesilwanyana | Januwari 0.75 | 1. Ukuthintela ukuguquka kwamalungu e-tibial, ukuphazamiseka kokuhamba "komqolo ogobileyo", ukuxengaxenga, umonakalo wemisipha yentliziyo; 2. Thintela ukubola kweenwele okanye uboya, zibe ziinwele eziqinileyo, ulahlekelwe kukugoba okuqhelekileyo, uthintele ukuvela "kwamabala angwevu" kwisangqa samehlo; 3. Ukuthintela ukwehla kobunzima, urhudo, ukuveliswa kobisi Ukuncipha. |
2. Udidi lokutya lweFerrous Amino Acid Chelate
- Igama leMveliso: I-Ferrous Amino Acid Chelate Feed Grade
- Inkangeleko: Iigranule eziluhlaza ezimdaka
- Iiparamitha zefiziksikhemikhali
a) Isinyithi: ≥ 10.0%
b) Ii-amino acids zizonke: ≥ 19.0%
c) Izinga le-Chelation: ≥ 95%
d) I-Arsenic: ≤ 2 mg/kg
e) I-Lead: ≤ 5 mg/kg
f) I-Cadmium: ≤ 5 mg/kg
g) Umxholo wokufuma: ≤ 5.0%
h) Ubunono: Zonke iisuntswana zidlula kwi-mesh ezingama-20, kunye nobukhulu beesuntswana eziyintloko eziyi-mesh ezingama-60-80
n=0,1,2,...ibonisa i-chelated zinc kwii-dipeptides, ii-tripeptides, kunye nee-tetrapeptides
Iimpawu zeFerrous Amino Acid Chelate Feed Grade
- Le mveliso yiminerali enomkhondo wendalo e-chelated yinkqubo ekhethekileyo ye-chelating ene-enzyme yezityalo ezicocekileyo, iipeptides ezincinci ze-molecule njenge-chelating substrates kunye nezinto ezinomkhondo;
- Le mveliso izinzile ngokweekhemikhali kwaye inokunciphisa kakhulu umonakalo wayo kwiivithamini namafutha, njl. Ukusetyenziswa kwale mveliso kunceda ekuphuculeni umgangatho wesondlo;
- Imveliso ifunxwa ngeendlela ezincinci zepeptide kunye ne-amino acid, inciphisa ukhuphiswano kunye nokuchasana nezinye izinto ezincinci, kwaye inezinga eliphezulu lokufunxwa kunye nokusetyenziswa kwezinto eziphilayo;
- Le mveliso ingadlula kumqobo we-placenta kunye ne-mammary gland, yenze umntwana ongekazalwa abe sempilweni, yonyuse ubunzima bokuzalwa kunye nobunzima bokulunyulwa, kwaye inciphise izinga lokufa; I-iron yinxalenye ebalulekileyo ye-hemoglobin kunye ne-myoglobin, enokuthi ithintele ngempumelelo i-anemia yokunqongophala kwe-iron kunye neengxaki zayo.
Ukusetyenziswa kunye nokusebenza kakuhle kweFerrous Amino Acid Chelate Feed Grade
| Into yesicelo | Idosi ecetyiswayo (izinto ezixabisekileyo ngokupheleleyo ze-g/t) | Umxholo kwi-feed epheleleyo (mg/kg) | Ukusebenza kakuhle |
| Hlwayela | 300～800 | 45～120 | 1. Ukuphucula ukusebenza kokuzala kunye nobomi bokusetyenziswa kweemazi; 2. ukuphucula ubunzima bokuzalwa, ubunzima bokulunyulwa kunye nokufana kwehagu ukuze ivelise ngcono kwixesha elizayo; 3. Ukuphucula ukugcinwa kwesinyithi kwiihagu ezincancisayo kunye nobuninzi besinyithi kubisi ukuthintela i-anemia yokunqongophala kwesinyithi kwiihagu ezincancisayo. |
| Amantshontsho eehagu kunye neehagu ezityetyisiweyo | Amantshontsho eehagu angama-300～600 | 45～90 | 1. Ukuphucula amajoni omzimba eehagu, ukonyusa ukumelana nesifo kunye nokuphucula izinga lokusinda; 2. Ukwandisa izinga lokukhula, ukuphucula ukuguqulwa kokutya, ukwandisa ubunzima bokulunyulwa kweentsana kunye nokufana kwazo, kunye nokunciphisa ukwanda kwezifo zeehagu; 3. Ukuphucula inqanaba le-myoglobin kunye ne-myoglobin, ukuthintela nokunyanga i-anemia yokunqongophala kwe-iron, ukwenza ulusu lwehagu lube bomvu kwaye ngokucacileyo kuphucule umbala wenyama. |
| Iihagu ezityebisayo 200～400 | 30～60 | ||
| Intaka | 300～400 | 45～60 | 1. Ukuphucula ukuguqulwa kokutya, ukwandisa izinga lokukhula, ukuphucula amandla okulwa noxinzelelo kunye nokunciphisa ukufa; 2. Phucula izinga lokubeka amaqanda, nciphisa izinga lokwaphuka kwamaqanda kwaye ujike umbala womthubi; 3. Ukuphucula izinga lokuchumisa kunye nezinga lokuqandusela kwamaqanda okuzala kunye nezinga lokusinda kweenkukhu eziselula. |
| Izilwanyana zasemanzini | 200～300 | 30～45 | 1. Khuthaza ukukhula, phucula ukuguqulwa kokutya; 2. Ukuphucula amandla okulwa noxinzelelo, ukunciphisa ukugula nokufa. |
3. Ibanga lokutya le-Zinc Amino Acid Chelate
- Igama leMveliso: Ibanga lokutya leZinc Amino Acid Chelate
- Inkangeleko: iigranules ezimdaka-ezimthubi
- Iiparamitha zefiziksikhemikhali
a) I-Zinc: ≥ 10.0%
b) Ii-amino acids zizonke: ≥ 20.5%
c) Izinga le-Chelation: ≥ 95%
d) I-Arsenic: ≤ 2 mg/kg
e) I-Lead: ≤ 5 mg/kg
f) I-Cadmium: ≤ 5 mg/kg
g) Umxholo wokufuma: ≤ 5.0%
h) Ubunono: Zonke iisuntswana zidlula kwi-mesh ezingama-20, kunye nobukhulu beesuntswana eziyintloko eziyi-mesh ezingama-60-80
n=0,1,2,...ibonisa i-chelated zinc kwii-dipeptides, ii-tripeptides, kunye nee-tetrapeptides
Iimpawu zeZinc Amino Acid Chelate Feed Grade
Le mveliso yiminerali ephilayo yonke e-chelating eyenziwe ngenkqubo ekhethekileyo ye-chelating ene-enzyme yezityalo ezincinci ze-peptides njenge-chelating substrates kunye nezinto ezilandelelanayo;
Le mveliso izinzile ngokweekhemikhali kwaye inokunciphisa kakhulu umonakalo wayo kwiivithamini kunye namafutha, njl.
Ukusetyenziswa kwale mveliso kuyanceda ekuphuculeni umgangatho wesondlo; Le mveliso ifunxwa ngeendlela ezincinci zepeptide kunye ne-amino acid, inciphisa ukhuphiswano kunye nokuchasana nezinye izinto ezincinci, kwaye inezinga eliphezulu lokufunxwa kunye nokusetyenziswa kwe-bio;
Le mveliso inokuphucula amajoni omzimba, ikhuthaze ukukhula, inyuse ukuguqulwa kokutya kwaye iphucule ukukhazimla koboya;
I-Zinc yinxalenye ebalulekileyo yee-enzymes ezingaphezu kwama-200, izicubu ze-epithelial, i-ribose kunye ne-gustatin. Ikhuthaza ukwanda ngokukhawuleza kweeseli ze-tastebud kwi-mucosa yolwimi kwaye ilawula inkanuko yokutya; ithintela iintsholongwane eziyingozi zamathumbu; kwaye inomsebenzi wee-antibiotics, ezinokuphucula umsebenzi wokukhupha inkqubo yokugaya ukutya kunye nomsebenzi wee-enzymes kwizicubu nakwiiseli.
Ukusetyenziswa kunye nokusebenza kakuhle kweZinc Amino Acid Chelate Feed Grade
| Into yesicelo | Idosi ecetyiswayo (izinto ezixabisekileyo ngokupheleleyo ze-g/t) | Umxholo kwi-feed epheleleyo (mg/kg) | Ukusebenza kakuhle |
| Iimazi ezikhulelweyo nezincancisayo | 300～500 | 45～75 | 1. Ukuphucula ukusebenza kokuzala kunye nobomi bokusetyenziswa kweemazi; 2. Ukuphucula amandla emveku kunye namantshontsho eehagu, kuphucula ukumelana nezifo, kwaye kubenze babe nokusebenza ngcono kwemveliso kwinqanaba lokugqibela; 3. Ukuphucula imeko yomzimba yeemazi ezimithiyo kunye nobunzima bokuzalwa kweehagu. |
| Ihagu encancisayo, ihagu encinci kunye neehagu ezikhulisayo | 250～400 | 37.5～60 | 1. Ukuphucula amajoni omzimba eehagu, ukunciphisa urhudo kunye nokufa; 2. Ukuphucula ukutyeba kakuhle, ukwandisa ukutya okutyiwayo, ukwandisa izinga lokukhula kunye nokuphucula ukuguqulwa kokutya; 3. Yenza uboya behagu bukhanye kwaye uphucule umgangatho wesidumbu kunye nomgangatho wenyama. |
| Intaka | 300～400 | 45～60 | 1. Phucula ukukhazimla kweentsiba; 2. ukuphucula izinga lokubeka amaqanda, izinga lokuchumisa kunye nezinga lokuqandusela amaqanda, kunye nokuqinisa amandla okufaka imibala kwiqanda eliyingqayi; 3. Ukuphucula amandla okulwa noxinzelelo kunye nokunciphisa ukufa; 4. Ukuphucula ukuguqulwa kokutya kunye nokwandisa izinga lokukhula. |
| Izilwanyana zasemanzini | NgoJanuwari 300 | 45 | 1. Khuthaza ukukhula, phucula ukuguqulwa kokutya; 2. Ukuphucula amandla okulwa noxinzelelo, ukunciphisa ukugula nokufa. |
| Isilwanyana esizingelayo g/intloko yesilwanyana | 2.4 | 1. Ukuphucula isivuno sobisi, ukuthintela i-mastitis kunye nokubola kwefoof, kunye nokunciphisa umxholo weeseli zomzimba kubisi; 2. Khuthaza ukukhula, uphucule ukuguqulwa kokutya kunye nokuphucula umgangatho wenyama. |
4. Ibanga lokutya leManganese Amino Acid Chelate
- Igama leMveliso: Ibanga lokutya leManganese Amino Acid Chelate
- Inkangeleko: iigranules ezimdaka-ezimthubi
- Iiparamitha zefiziksikhemikhali
a) Mn: ≥ 10.0%
b) Ii-amino acids zizonke: ≥ 19.5%
c) Izinga le-Chelation: ≥ 95%
d) I-Arsenic: ≤ 2 mg/kg
e) I-Lead: ≤ 5 mg/kg
f) I-Cadmium: ≤ 5 mg/kg
g) Umxholo wokufuma: ≤ 5.0%
h) Ubunono: Zonke iisuntswana zidlula kwi-mesh ezingama-20, kunye nobukhulu beesuntswana eziyintloko eziyi-mesh ezingama-60-80
n=0, 1,2,...ibonisa i-chelated manganese kwii-dipeptides, ii-tripeptides, kunye nee-tetrapeptides
Iimpawu zeManganese Amino Acid Chelate Feed Grade
Le mveliso yiminerali ephilayo yonke e-chelating eyenziwe ngenkqubo ekhethekileyo ye-chelating ene-enzyme yezityalo ezincinci ze-peptides njenge-chelating substrates kunye nezinto ezilandelelanayo;
Le mveliso izinzile ngokweekhemikhali kwaye inokunciphisa kakhulu umonakalo wayo kwiivithamini namafutha, njl. Ukusetyenziswa kwale mveliso kunceda ekuphuculeni umgangatho wesondlo;
Imveliso ifunxwa ngeendlela ezincinci zepeptide kunye ne-amino acid, inciphisa ukhuphiswano kunye nokuchasana nezinye izinto ezincinci, kwaye inezinga eliphezulu lokufunxwa kunye nokusetyenziswa kwezinto eziphilayo;
Le mveliso inokuphucula izinga lokukhula, iphucule ukuguqulwa kokutya kunye nemeko yempilo kakhulu; kwaye iphucule izinga lokuzala, izinga lokuqandusela kunye nezinga elisempilweni leenkuku zokuzala; ngokucacileyo;
I-Manganese iyimfuneko ekukhuleni kwamathambo nasekugcinweni kwezicubu ezidityanisiweyo. Inxulumene kakhulu nee-enzymes ezininzi; kwaye ithatha inxaxheba kwi-carbohydrate, amafutha kunye ne-protein metabolism, ukuzala kunye nempendulo yomzimba yokuzikhusela.
Ukusetyenziswa kunye nokusebenza kakuhle kweManganese Amino Acid Chelate Feed Grade
| Into yesicelo | Idosi ecetyiswayo (izinto ezixabisekileyo ngokupheleleyo ze-g/t) | Umxholo kwi-feed epheleleyo (mg/kg) | Ukusebenza kakuhle |
| Ihagu yokuzalisa | 200～300 | 30～45 | 1. Ukukhuthaza uphuhliso oluqhelekileyo lwamalungu esini kunye nokuphucula ukuhamba kwesidoda; 2. Ukuphucula amandla okuzala eehagu ezizalayo kunye nokunciphisa imiqobo yokuzala. |
| Amantshontsho eehagu kunye neehagu ezityetyisiweyo | 100～250 | 15～37.5 | 1. Kuluncedo ukuphucula imisebenzi yomzimba yokuzikhusela, kunye nokuphucula amandla okulwa noxinzelelo kunye nokumelana nezifo; 2. Khuthaza ukukhula nokuphucula ukuguqulwa kokutya kakhulu; 3. Phucula umbala wenyama kunye nomgangatho wayo, kwaye uphucule ipesenti yenyama engenamafutha. |
| Intaka | 250～350 | 37.5～52.5 | 1. Ukuphucula amandla okulwa noxinzelelo kunye nokunciphisa ukufa; 2. Ukuphucula izinga lokubeka amaqanda, izinga lokuchumisa kunye nezinga lokuqandusela amaqanda, ukuphucula umgangatho wamaqokobhe amaqanda kunye nokunciphisa izinga lokuqhekeka kwamaqokobhe; 3. Khuthaza ukukhula kwamathambo kwaye unciphise ukwanda kwezifo zemilenze. |
| Izilwanyana zasemanzini | 100～200 | 15～30 | 1. Khuthaza ukukhula kwaye uphucule amandla ayo okulwa noxinzelelo kunye nokumelana nezifo; 2. Ukuphucula ukuhamba kwesidoda kunye nesantya sokuqanduselwa kwamaqanda aqhamkileyo. |
| Isilwanyana esizingelayo g/intloko yesilwanyana | Iinkomo 1.25 | 1. Ukuthintela ukuphazamiseka kokwenziwa kwe-fatty acid kunye nomonakalo wezicubu zamathambo; 2. Ukuphucula amandla okuzala, ukuthintela ukuphunza kunye nokukhubazeka kwezilwanyana eziziimazi emva kokubeleka, ukunciphisa ukufa kwamathole kunye namatakane, kwaye wonyuse ubunzima bezilwanyana ezisandul’ ukuzalwa. | |
| Ibhokhwe 0.25 |
Icandelo 6 I-FAB yeChelates yePeptide encinci-yemineral
| S/N | F: Iimpawu ezisebenzayo | A: Umahluko kukhuphiswano | B: Iingenelo eziziswa kukungafani kokhuphiswano kubasebenzisi |
| 1 | Ulawulo lokukhetha izinto eziluhlaza | Khetha i-hydrolysis ye-enzyme yesityalo esicocekileyo yeepeptides ezincinci | Ukhuseleko oluphezulu lwebhayoloji, ukuphepha ukutya abantu |
| 2 | Itekhnoloji yokugaya ekhokelayo ye-enzyme yebhayoloji ephindwe kabini | Inani eliphezulu leepeptides ezincinci zemolekyuli | "Iithagethi" ezingaphezulu, ezingelula ukuzigcwalisa, ezinemisebenzi ephezulu yebhayoloji kunye nozinzo olungcono |
| 3 | Itekhnoloji yokutshiza nokomisa uxinzelelo ephucukileyo | Imveliso yegranular, enobukhulu obufanayo besuntswana, ukunyibilika okungcono, akukho lula ukufunxa ukufuma | Qinisekisa ukuba kulula ukuyisebenzisa, ukuxuba okufanayo kwisondlo esipheleleyo |
| Umthamo wamanzi ophantsi (≤ 5%), nto leyo enciphisa kakhulu impembelelo ebangelwa ziivithamini kunye namalungiselelo ee-enzyme | Ukuphucula uzinzo lweemveliso zokutya | ||
| 4 | Itekhnoloji yokulawula imveliso ephucukileyo | Inkqubo evalelwe ngokupheleleyo, inqanaba eliphezulu lolawulo oluzenzekelayo | Umgangatho okhuselekileyo nozinzileyo |
| 5 | Itekhnoloji yokulawula umgangatho ephucukileyo | Misela kwaye uphucule iindlela zesayensi neziphambili zohlalutyo kunye neendlela zokulawula zokufumanisa izinto ezichaphazela umgangatho wemveliso, ezinje ngeproteni enyibilikayo kwi-asidi, ukusasazwa kobunzima bemolekyuli, ii-amino acids kunye nesantya se-chelating | Qinisekisa umgangatho, qinisekisa ukusebenza kakuhle kwaye uphucule ukusebenza kakuhle |
Icandelo 7 Uthelekiso loMkhuphisani
Umgangatho oQhelekileyo we-VS
Uthelekiso lokusasazwa kwe-peptide kunye nezinga le-chelation yeemveliso
| Iimveliso zikaSustar | Ubungakanani beepeptides ezincinci (180-500) | Iimveliso zeZinpro | Ubungakanani beepeptides ezincinci (180-500) |
| I-AA-Cu | ≥74% | I-AVAILA-Cu | 78% |
| I-AA-Fe | ≥48% | IFUMANEKA-FE | 59% |
| I-AA-Mn | ≥33% | IFUMANEKA-NGOMN | 53% |
| I-AA-Zn | ≥37% | I-AVAILA-Zn | 56% |
| Iimveliso zikaSustar | Izinga leChelation | Iimveliso zeZinpro | Izinga leChelation |
| I-AA-Cu | 94.8% | I-AVAILA-Cu | 94.8% |
| I-AA-Fe | 95.3% | IFUMANEKA-FE | 93.5% |
| I-AA-Mn | 94.6% | IFUMANEKA-NGOMN | 94.6% |
| I-AA-Zn | 97.7% | I-AVAILA-Zn | 90.6% |
Umlinganiselo weepeptides ezincinci zeSustar uphantsi kancinci kunoweZinpro, kwaye izinga le-chelation leemveliso zeSustar liphezulu kancinci kunoweemveliso zeZinpro.
Uthelekiso lomxholo wee-amino acid ezili-17 kwiimveliso ezahlukeneyo
| Igama lika ii-amino acids | Ubhedu lukaSustar I-Amino Acid Chelate Ibanga lokutya | IZinpro's IYAFUMANEKA ithusi | I-Sustar's Ferrous Amino Acid C i-helate Feed Ibanga | I-Zinpro's IYAFUMANEKA isinyithi | I-Manganese kaSustar I-Amino Acid Chelate Ibanga lokutya | I-Zinpro's IYAFUMANEKA i-manganese | I-Sustar's Zinc I-Amino Acid Ibanga lokutya leChelate | I-Zinpro's IYAFUMANEKA izinki |
| i-aspartic acid (%) | 1.88 | 0.72 | 1.50 | 0.56 | 1.78 | 1.47 | 1.80 | 2.09 |
| i-glutamic acid (%) | 4.08 | 6.03 | 4.23 | 5.52 | 4.22 | 5.01 | 4.35 | 3.19 |
| I-Serine (%) | 0.86 | 0.41 | 1.08 | 0.19 | 1.05 | 0.91 | 1.03 | 2.81 |
| I-Histidine (%) | 0.56 | 0.00 | 0.68 | 0.13 | 0.64 | 0.42 | 0.61 | 0.00 |
| I-Glycine (%) | 1.96 | 4.07 | 1.34 | 2.49 | 1.21 | 0.55 | 1.32 | 2.69 |
| I-Threonine (%) | 0.81 | 0.00 | 1.16 | 0.00 | 0.88 | 0.59 | 1.24 | 1.11 |
| I-Arginine (%) | 1.05 | 0.78 | 1.05 | 0.29 | 1.43 | 0.54 | 1.20 | 1.89 |
| I-Alanine (%) | 2.85 | 1.52 | 2.33 | 0.93 | 2.40 | 1.74 | 2.42 | 1.68 |
| I-Tyrosinase (%) | 0.45 | 0.29 | 0.47 | 0.28 | 0.58 | 0.65 | 0.60 | 0.66 |
| I-Cystinol (%) | 0.00 | 0.00 | 0.09 | 0.00 | 0.11 | 0.00 | 0.09 | 0.00 |
| I-Valine (%) | 1.45 | 1.14 | 1.31 | 0.42 | 1.20 | 1.03 | 1.32 | 2.62 |
| I-Methionine (%) | 0.35 | 0.27 | 0.72 | 0.65 | 0.67 | 0.43 | Januwari 0.75 | 0.44 |
| I-Phenylalanine (%) | 0.79 | 0.41 | 0.82 | 0.56 | 0.70 | 1.22 | 0.86 | 1.37 |
| I-Isoleucine (%) | 0.87 | 0.55 | 0.83 | 0.33 | 0.86 | 0.83 | 0.87 | 1.32 |
| I-Leucine (%) | 2.16 | 0.90 | 2.00 | 1.43 | 1.84 | 3.29 | 2.19 | 2.20 |
| I-Lysine (%) | 0.67 | 2.67 | 0.62 | 1.65 | 0.81 | 0.29 | 0.79 | 0.62 |
| I-Proline (%) | 2.43 | 1.65 | 1.98 | 0.73 | 1.88 | 1.81 | 2.43 | 2.78 |
| Ii-amino acids zizonke (%) | 23.2 | 21.4 | 22.2 | 16.1 | 22.3 | 20.8 | 23.9 | 27.5 |
Lilonke, umlinganiselo wee-amino acids kwiimveliso zeSustar uphezulu kunalowo ukwimveliso zeZinpro.
Icandelo 8 Imiphumo yokusetyenziswa
Imiphumo yemithombo eyahlukeneyo yeeminerali ezilandelelanayo kwimveliso kunye nomgangatho wamaqanda eenkukhu ezibeka amaqanda kwixesha lokugqibela lokubeka amaqanda
Inkqubo yeMveliso
- Itekhnoloji ye-chelation ekujoliswe kuyo
- Itekhnoloji yokuxuba i-shear
- Itekhnoloji yokutshiza nokomisa ngoxinzelelo
- Itekhnoloji yokufakela efrijini kunye nokususa ubumanzi
- Itekhnoloji yokulawula okusingqongileyo ephucukileyo
Isihlomelo A: Iindlela zokuMisela ukusasazwa kwe-peptides ngobunzima beemolekyuli
Ukwamkelwa komgangatho: GB/T 22492-2008
1 Umgaqo woVavanyo:
Yachongwa yi-chromatography ye-gel filtration esebenza kakhulu. Oko kukuthi, kusetyenziswa i-porous filler njenge-stationary phase, ngokusekelwe kumahluko kubungakanani be-molecular mass yee-sample components zokwahlulwa, ezifunyenwe kwi-peptide bond ye-ultraviolet absorption wavelength ye-220nm, kusetyenziswa isoftware yokucubungula idatha ezinikeleyo yokumisela ukusasazwa kwe-molecule mass nge-gel filtration chromatography (oko kukuthi, isoftware ye-GPC), ii-chromatograms kunye nedatha yazo zacutshungulwa, zabalwa ukuze kufunyanwe ubungakanani be-molecule mass ye-soybean peptide kunye noluhlu lokusasazwa.
2. Ii-reagents
Amanzi ovavanyo kufuneka ahlangabezane nenkcazo yamanzi esibini kwi-GB/T6682, ukusetyenziswa kwee-reagents, ngaphandle kwemigaqo ekhethekileyo, kucocekile ngokweenkcazo.
2.1 Izinto ezisetyenziswayo ziquka i-acetonitrile (ecocekileyo ngokwe-chromatographic), i-trifluoroacetic acid (ecocekileyo ngokwe-chromatographic),
2.2 Izinto eziqhelekileyo ezisetyenziswa kwi-calibration curve yokusasazwa kobunzima be-molecular: i-insulin, i-mycopeptides, i-glycine-glycine-tyrosine-arginine, i-glycine-glycine-glycine
3 Izixhobo nezixhobo
3.1 I-Chromatograph yoLwakhiwo oluSebenza ngokuPhezulu (i-HPLC): i-workstation okanye i-integrator ye-chromatographic ene-UV detector kunye nesoftware yokucubungula idatha ye-GPC.
3.2 Iyunithi yokucoca kunye nokukhupha igesi kwi-vacuum phase mobile phase.
3.3 Ibhalansi ye-elektroniki: ixabiso eligqityiweyo 0.000 1g.
Amanyathelo okusebenza ama-4
4.1 Iimeko zeChromatographic kunye novavanyo lohlengahlengiso lwenkqubo (iimeko zesalathiso)
4.1.1 Ikholamu yeChromatographic: TSKgelG2000swxl300 mm×7.8 mm (ububanzi bangaphakathi) okanye ezinye iikholamu zejeli zohlobo olufanayo ezinentsebenzo efanayo efanelekileyo ekumiselweni kweeproteni kunye neepeptides.
4.1.2 Isigaba sokuhamba: I-Acetonitrile + amanzi + i-trifluoroacetic acid = 20 + 80 + 0.1.
4.1.3 Ubude bomda wokufumanisa: 220 nm.
4.1.4 Isantya sokuhamba kwamanzi: 0.5 mL/min.
4.1.5 Ixesha lokufumanisa: imizuzu engama-30.
4.1.6 Umthamo wesampuli yokujova: 20μL.
4.1.7 Ubushushu bekholamu: ubushushu begumbi.
4.1.8 Ukuze inkqubo ye-chromatographic ihlangabezane neemfuno zokufumanisa, kwacaciswa ukuba phantsi kweemeko ze-chromatographic ezingentla, ukusebenza kakuhle kwekholamu ye-gel chromatographic, oko kukuthi, inani leeplate (N), belingaphantsi kwe-10000 elibalwe ngokusekelwe kwiincopho zomgangatho we-tripeptide (iGlycine-Glycine-Glycine).
4.2 Ukuveliswa kwee-curves ezisemgangathweni zobunzima be-molecular
Izisombululo ezisemgangathweni zepeptide ezisemgangathweni ze-molecule mass ezingentla ezahlukeneyo ezine-mass concentration ye-1 mg / mL zilungiselelwe ngokuhambelana kwe-mobile phase, zixutywe kwi-ratio ethile, zaze zahluzwa nge-organic phase membrane enobukhulu be-pore obuyi-0.2 μm ~ 0.5 μm zaza zafakwa kwisampuli, kwaza kwafunyanwa ii-chromatograms zemigangatho. Ii-relative molecular mass calibration curves kunye ne-equation zazo zifunyenwe ngokudwelisa i-logarithm ye-relative molecular mass ngokuchasene nexesha lokugcinwa okanye nge-linear regression.
4.3 Unyango lwesampulu
Linganisa ngokuchanekileyo i-10mg yesampulu kwiflaski yevolumu ye-10mL, yongeza i-mobile phase encinci, i-ultrasonic shake imizuzu eyi-10, ukuze isampulu inyibilike ngokupheleleyo kwaye ixutywe, ixutywe ne-mobile phase ukuya kwisikali, ize ihluzwe nge-organic phase membrane enobukhulu be-pore obuyi-0.2μm ~ 0.5μm, kwaye i-filtrate ihlalutywe ngokweemeko ze-chromatographic kwi-A.4.1.
5. Ukubalwa kokusasazwa kobunzima be-molecular
Emva kokuhlalutya isisombululo sesampulu esilungiselelwe kwi-4.3 phantsi kweemeko ze-chromatographic ze-4.1, ubunzima beemolekyuli ezihambelanayo zesampulu kunye noluhlu lwazo lokusasazwa zinokufunyanwa ngokufaka idatha ye-chromatographic yesampulu endaweni ye-calibration curve 4.2 ngesoftware yokucubungula idatha ye-GPC. Ukusasazwa kobunzima beemolekyuli ezihambelanayo zeepeptide ezahlukeneyo kunokubalwa ngendlela yokuqheleka kwendawo ende, ngokwefomula: X=A/A iyonke×100
Kwifomyula: X - Inxalenye yobunzima be-peptide yobunzima be-molecular kwi-peptide iyonke kwisampuli, %;
A - Indawo encochoyiweyo yepeptide enobunzima bemolekyuli;
Isimbuku A - isimbuku seendawo eziphakamileyo zepeptide nganye ye-molecular mass, ebalwe kwindawo enye yedesimali.
6 Ukuphindaphinda
Umahluko opheleleyo phakathi kwezigqibo ezimbini ezizimeleyo ezifunyenwe phantsi kweemeko zokuphindaphindeka akufuneki udlule i-15% yentsingiselo yezibalo zezigqibo ezimbini.
Isihlomelo B: Iindlela zokuMiselwa kwee-Amino Acids zasimahla
Ukwamkelwa komgangatho: Q/320205 KAVN05-2016
1.2 Izinto ezisetyenziswayo kunye nezinto ezisetyenziswayo
I-acetic acid ye-glacial: icocekile ngokweenkcukacha
I-Perchloric acid: 0.0500 mol/L
Isalathisi: Isalathisi se-crystal violet esingu-0.1% (i-glacial acetic acid)
2. Ukumiselwa kwee-amino acids zasimahla
Iisampulu zomiswe kwi-80°C kangangeyure e-1.
Beka isampuli kwisitya esomileyo ukuze iphole ngokwendalo ukuya kubushushu begumbi okanye iphole ukuya kubushushu obufanelekileyo.
Bulisa malunga ne-0.1 g yesampulu (echanekileyo ukuya kwi-0.001 g) kwiflaski eyomileyo eyi-250 mL.
Qhubela phambili ngokukhawuleza uye kwinqanaba elilandelayo ukuze uphephe ukuba isampuli ingafunxi umswakama ongqongileyo
Yongeza i-25 mL ye-glacial acetic acid uze udibanise kakuhle ungadluli kwimizuzu emi-5.
Yongeza amaconsi amabini e-crystal violet indicator
I-Titrate enesisombululo se-0.0500 mol / L (±0.001) se-titration esiqhelekileyo se-perchloric acid de isisombululo sitshintshe ukusuka kwi-purple ukuya kwi-end point.
Bhala phantsi umthamo wesisombululo esiqhelekileyo esisetyenzisiweyo.
Yenza uvavanyo olungenanto ngaxeshanye.
3. Ukubala kunye neziphumo
Umxholo we-amino acid wasimahla u-X kwi-reagent uchazwa njengeqhekeza elinobunzima (%) kwaye ubalwa ngokwefomula: X = C × (V1-V0) × 0.1445/M × 100%, kwifomula ye-tne:
C - Uxinzelelo lwesisombululo esiqhelekileyo se-perchloric acid kwii-moles ngelitha (mol/L)
V1 - Umthamo osetyenziselwa ukuhluzwa kweesampuli ngesisombululo esiqhelekileyo se-perchloric acid, kwi-milliliters (mL).
I-Vo - Umthamo osetyenziselwa i-titration engenanto kunye nesisombululo esiqhelekileyo se-perchloric acid, kwi-milliliters (mL);
M - Ubunzima besampuli, ngeegrama (g).
0.1445: Ubunzima obuqhelekileyo bee-amino acids bulingana ne-1.00 mL yesisombululo esiqhelekileyo se-perchloric acid [c (HClO4) = 1.000 mol / L].
Isihlomelo C: Iindlela zokuMisela izinga le-chelation likaSustar
Ukwamkelwa kwemigangatho: Q/70920556 71-2024
1. Umgaqo wokuzimisela (uFe njengomzekelo)
Ii-amino acid iron complexes zinyibilika kancinci kakhulu kwi-anhydrous ethanol kwaye ii-free metal ions ziyanyibilika kwi-anhydrous ethanol, umahluko wokunyibilika phakathi kwezi zimbini kwi-anhydrous ethanol wasetyenziswa ukumisela izinga le-chelation yee-amino acid iron complexes.
2. IiReagents kunye neZisombululo
I-ethanol engenamanzi; okuseleyo kuyafana nesiqendu 4.5.2 kwi-GB/T 27983-2011.
3. Amanyathelo ohlalutyo
Yenza uvavanyo oluphindwe kabini ngaxeshanye. Linganisa i-0.1g yesampulu eyomileyo kwi-103±2℃ iyure e-1, ichaneke kwi-0.0001g, yongeza i-100mL ye-ethanol engenamanzi ukuze inyibilike, hluza, hluza intsalela ehlanjwe nge-100mL ye-ethanol engenamanzi ubuncinane izihlandlo ezithathu, uze udlulisele intsalela kwi-flask ye-conical ye-250mL, yongeza i-10mL yesisombululo se-sulfuric acid ngokwesiqendu 4.5.3 kwi-GB/T27983-2011, uze wenze la manyathelo alandelayo ngokwesiqendu 4.5.3 esithi “Fudumeza ukuze unyibilike uze uyivumele iphole” kwi-GB/T27983-2011. Yenza uvavanyo olungenanto ngaxeshanye.
4. Ukumiselwa komxholo wesinyithi uwonke
4.1 Umgaqo wokumisela uyafana nomhlathi 4.4.1 kwi-GB/T 21996-2008.
4.2. Izinto ezivuselelayo kunye nezisombululo
4.2.1 I-asidi exutyiweyo: Yongeza i-150mL ye-sulfuric acid kunye ne-150mL ye-phosphoric acid kwi-700mL yamanzi uze udibanise kakuhle.
4.2.2 Isisombululo sesalathisi se-Sodium diphenylamine sulfonate: 5g/L, silungiselelwe ngokwe-GB/T603.
4.2.3 Isisombululo se-titration esisemgangathweni se-Cerium sulfate: i-concentration c [Ce (SO4) 2] = 0.1 mol/L, esilungisiweyo ngokwe-GB/T601.
4.3 Amanyathelo ohlalutyo
Yenza uvavanyo oluphindwe kabini ngaxeshanye. Linganisa i-0.1g yesampulu, echanekileyo kwi-020001g, yibeke kwiflaski yekhonikhi ye-250mL, yongeza i-10mL ye-asidi exutyiweyo, emva kokunyibilika, yongeza i-30ml yamanzi kunye namaconsi ama-4 esisombululo se-sodium dianiline sulfonate indicator, uze wenze la manyathelo alandelayo ngokwesiqendu 4.4.2 kwi-GB/T21996-2008. Yenza uvavanyo olungenanto ngaxeshanye.
4.4 Ukubonakaliswa kweziphumo
Umxholo wesinyithi uwonke u-X1 we-amino acid iron complexes ngokwe-mass fraction yesinyithi, ixabiso elichazwe kwi-%, libalwe ngokwefomula (1):
X1=(V-V0)×C×M×10-3×100
Kwifomyula: V - umthamo wesisombululo esiqhelekileyo se-cerium sulfate esisetyenziswayo ukuze kuthathwe isisombululo sovavanyo, i-mL;
Isisombululo esiqhelekileyo se-cerium sulfate esisetyenziswayo ekulinganisweni kwesisombululo esingenanto, i-mL;
C - Uxinzelelo lokwenyani lwesisombululo esiqhelekileyo se-cerium sulfate, i-mol/L
5. Ukubalwa komxholo wesinyithi kwii-chelates
Umxholo wesinyithi u-X2 kwi-chelate ngokwenxalenye yobunzima besinyithi, ixabiso elichazwe kwi-%, libalwe ngokwefomula: x2 = ((V1-V2) × C × 0.05585)/m1 × 100
Kwifomyula: V1 - umthamo wesisombululo esiqhelekileyo se-cerium sulfate esisetyenziswayo ukuze kuthathwe isisombululo sovavanyo, i-mL;
Isisombululo esiqhelekileyo se-cerium sulfate esisetyenziselwa ukulinganisa isisombululo esingenanto, i-mL;
C - Uxinzelelo lokwenyani lwesisombululo esiqhelekileyo se-cerium sulfate, i-mol/L;
0.05585 - ubunzima bentsimbi yentsimbi evezwa kwiigrama ezilingana ne-1.00 mL yesisombululo esiqhelekileyo se-cerium sulfate C[Ce(SO4)2.4H20] = 1.000 mol/L.
m1-Ubunzima besampulu, g. Thatha i-arithmetic mean yeziphumo zokumisela ezihambelanayo njengeziphumo zokumisela, kwaye umahluko opheleleyo weziphumo zokumisela ezihambelanayo awudluli kwi-0.3%.
6. Ukubalwa kwezinga le-chelation
Izinga le-Chelation X3, ixabiso elichazwe kwi-%, X3 = X2/X1 × 100
Isihlomelo C: Iindlela zokuMisela izinga le-Zinpro's chelation
Ukwamkelwa komgangatho: Q/320205 KAVNO7-2016
1. Izinto ezisetyenziswayo kunye nezinto
a) I-glacial acetic acid: icocekile ngokwezibalo; b) I-Perchloric acid: 0.0500mol/L; c) Isalathisi: Isalathisi se-crystal violet esingu-0.1% (i-glacial acetic acid)
2. Ukumiselwa kwee-amino acids zasimahla
2.1 Iisampulu zomiswe kwi-80°C kangangeyure e-1.
2.2 Beka isampuli kwisitya esomileyo ukuze iphole ngokwendalo ukuya kubushushu begumbi okanye iphole ukuya kubushushu obufanelekileyo.
2.3 Bulala malunga ne-0.1 g yesampulu (echanekileyo ukuya kwi-0.001 g) kwi-flask eyomileyo eyi-250 mL ekhonkrithi
2.4 Qhubela phambili ngokukhawuleza uye kwinqanaba elilandelayo ukuze uphephe ukuba isampuli ingafunxi umswakama ongqongileyo.
2.5 Yongeza i-25mL ye-glacial acetic acid uze udibanise kakuhle ungadluli kwi-5 min.
2.6 Yongeza amathontsi ama-2 e-crystal violet indicator.
2.7 Titrate enesisombululo se-0.0500mol/L (±0.001) se-titration esiqhelekileyo se-perchloric acid de isisombululo sitshintshe ukusuka komfusa ukuya koluhlaza kangangemizuzwana eli-15 ngaphandle kokutshintsha umbala njengendawo yokugqibela.
2.8 Bhala phantsi umthamo wesisombululo esiqhelekileyo esisetyenzisiweyo.
2.9 Yenza uvavanyo olungenanto ngaxeshanye.
3. Ukubala kunye neziphumo
Umxholo we-amino acid ekhululekileyo u-X kwi-reagent uchazwa njengeqhezu elinobunzima (%), ubalwe ngokwefomula (1): X=C×(V1-V0) ×0.1445/M×100%........(1)
Kwifomyula: C - uxinaniso lwesisombululo se-perchloric acid esiqhelekileyo kwiimoles ngelitha nganye (mol/L)
V1 - Umthamo osetyenziselwa ukuhluzwa kweesampuli ngesisombululo esiqhelekileyo se-perchloric acid, kwi-milliliters (mL).
I-Vo - Umthamo osetyenziselwa i-titration engenanto kunye nesisombululo esiqhelekileyo se-perchloric acid, kwi-milliliters (mL);
M - Ubunzima besampuli, ngeegrama (g).
0.1445 - Ubunzima obuqhelekileyo bee-amino acids bulingana ne-1.00 mL yesisombululo esiqhelekileyo se-perchloric acid [c (HClO4) = 1.000 mol / L].
4. Ukubalwa kwezinga le-chelation
Izinga le-chelation lesampuli lichazwa njenge-mass fraction (%), libalwa ngokwefomula (2): izinga le-chelation = (umxholo we-amino acid iyonke - umxholo we-amino acid wasimahla)/umxholo we-amino acid iyonke×100%.
Ixesha leposi: Sep-17-2025
